Synthesis and microstructural control of nanocrystalline cuo via precipitation

Yuan Xiang Luo; Dan Li; Juan Yang

Synthesis and microstructural control of nanocrystalline cuo via precipitation

Yuan Xiang Luo^*, Dan Li, Juan Yang

^*Corresponding author for this work

Research output: Contribution to journal › Journal Article › peer-review

3 Citations (Scopus)

Abstract

The nanocrystalline CuO powders with different microstructure were prepared by precipitation method using Cu (NO₃)₂ as copper raw material, water or ethanol as dispersants, and NaOH or NaOH-Na ₂CO₃ as precipitates. The structure, particle size and morphology of resulting CuO powders were characterized by XRD and TEM. Results indicated that the microstructure of resulting CuO powders depends on calcining temperature, dispersants and precipitates. TEM photographs reveal that the CuO particles produced using water as dispersant are ellipsoids with good dispersity, while the CuO particles produced using ethanol as dispersant are spherical shape with better dispersity. Compared with NaOH as precipitate, the CuO particles produced using NaOH-Na₂CO₃ as precipitate are smaller, but more heavily agglomerated. In addition, the catalysis of the nanocrystalline CuO powders on NH₄ClO₄ is investigated.

Original language	English
Pages (from-to)	53-55
Number of pages	3
Journal	Huozhayao Xuebao/Chinese Journal of Explosives and Propellants
Volume	25
Issue number	3
Publication status	Published - 2002
Externally published	Yes

Keywords

Microstructure
Nanocrystalline cuo
Nh clo
Precipitation method

Access to Document

https://hdl.handle.net/1783.1/143266

Cite this

@article{8f12f4f1c96b461a895f03ead82e5544,

title = "Synthesis and microstructural control of nanocrystalline cuo via precipitation",

abstract = "The nanocrystalline CuO powders with different microstructure were prepared by precipitation method using Cu (NO3)2 as copper raw material, water or ethanol as dispersants, and NaOH or NaOH-Na 2CO3 as precipitates. The structure, particle size and morphology of resulting CuO powders were characterized by XRD and TEM. Results indicated that the microstructure of resulting CuO powders depends on calcining temperature, dispersants and precipitates. TEM photographs reveal that the CuO particles produced using water as dispersant are ellipsoids with good dispersity, while the CuO particles produced using ethanol as dispersant are spherical shape with better dispersity. Compared with NaOH as precipitate, the CuO particles produced using NaOH-Na2CO3 as precipitate are smaller, but more heavily agglomerated. In addition, the catalysis of the nanocrystalline CuO powders on NH4ClO4 is investigated.",

keywords = "Microstructure, Nanocrystalline cuo, Nh clo, Precipitation method",

author = "Luo, \{Yuan Xiang\} and Dan Li and Juan Yang",

year = "2002",

language = "English",

volume = "25",

pages = "53--55",

journal = "Huozhayao Xuebao/Chinese Journal of Explosives and Propellants",

issn = "1007-7812",

publisher = "China Ordnance Industry Corporation",

number = "3",

}

TY - JOUR

T1 - Synthesis and microstructural control of nanocrystalline cuo via precipitation

AU - Luo, Yuan Xiang

AU - Li, Dan

AU - Yang, Juan

PY - 2002

Y1 - 2002

N2 - The nanocrystalline CuO powders with different microstructure were prepared by precipitation method using Cu (NO3)2 as copper raw material, water or ethanol as dispersants, and NaOH or NaOH-Na 2CO3 as precipitates. The structure, particle size and morphology of resulting CuO powders were characterized by XRD and TEM. Results indicated that the microstructure of resulting CuO powders depends on calcining temperature, dispersants and precipitates. TEM photographs reveal that the CuO particles produced using water as dispersant are ellipsoids with good dispersity, while the CuO particles produced using ethanol as dispersant are spherical shape with better dispersity. Compared with NaOH as precipitate, the CuO particles produced using NaOH-Na2CO3 as precipitate are smaller, but more heavily agglomerated. In addition, the catalysis of the nanocrystalline CuO powders on NH4ClO4 is investigated.

AB - The nanocrystalline CuO powders with different microstructure were prepared by precipitation method using Cu (NO3)2 as copper raw material, water or ethanol as dispersants, and NaOH or NaOH-Na 2CO3 as precipitates. The structure, particle size and morphology of resulting CuO powders were characterized by XRD and TEM. Results indicated that the microstructure of resulting CuO powders depends on calcining temperature, dispersants and precipitates. TEM photographs reveal that the CuO particles produced using water as dispersant are ellipsoids with good dispersity, while the CuO particles produced using ethanol as dispersant are spherical shape with better dispersity. Compared with NaOH as precipitate, the CuO particles produced using NaOH-Na2CO3 as precipitate are smaller, but more heavily agglomerated. In addition, the catalysis of the nanocrystalline CuO powders on NH4ClO4 is investigated.

KW - Microstructure

KW - Nanocrystalline cuo

KW - Nh clo

KW - Precipitation method

UR - https://www.scopus.com/pages/publications/33747082817

M3 - Journal Article

SN - 1007-7812

VL - 25

SP - 53

EP - 55

JO - Huozhayao Xuebao/Chinese Journal of Explosives and Propellants

JF - Huozhayao Xuebao/Chinese Journal of Explosives and Propellants

IS - 3

ER -

Synthesis and microstructural control of nanocrystalline cuo via precipitation

Abstract

Keywords

Access to Document

Other files and links

Fingerprint

Cite this