Synthesis of large optically clear SAPO-47 single crystals using n-propylamine as template

X. T. Xu; J. P. Zhai; Y. P. Chen; I. L. Li; S. C. Ruan; Z. K. Tang

doi:10.1016/j.jcrysgro.2015.05.029

Synthesis of large optically clear SAPO-47 single crystals using n-propylamine as template

X. T. Xu, J. P. Zhai^*, Y. P. Chen, I. L. Li, S. C. Ruan, Z. K. Tang

^*Corresponding author for this work

Research output: Contribution to journal › Journal Article › peer-review

8 Citations (Scopus)

Abstract

We report the hydrothermal synthesis of SAPO-47 crystals by using n-propylamine (NPA) as template. The resulting product sensitively depends on the gel compositions and synthesis procedure. By optimizing the molar ratio of SiO₂/Al₂O₃, content of HF and NPA, large perfect cubic-shaped SAPO-47 crystals are obtained (size 260 μm×260 μm), at a synthesis temperature of 200 °C with a crystallization of 50 h.

Original language	English
Pages (from-to)	123-128
Number of pages	6
Journal	Journal of Crystal Growth
Volume	426
DOIs	https://doi.org/10.1016/j.jcrysgro.2015.05.029
Publication status	Published - 22 Jun 2015
Externally published	Yes

Bibliographical note

Publisher Copyright:
© 2015 Elsevier B.V. All rights reserved.

Keywords

One-step temperature process
SAPO-47
Single crystals
n-Propylamine

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10.1016/j.jcrysgro.2015.05.029

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@article{879958bc10cf4d87ae1421247e5ee657,

title = "Synthesis of large optically clear SAPO-47 single crystals using n-propylamine as template",

abstract = "We report the hydrothermal synthesis of SAPO-47 crystals by using n-propylamine (NPA) as template. The resulting product sensitively depends on the gel compositions and synthesis procedure. By optimizing the molar ratio of SiO2/Al2O3, content of HF and NPA, large perfect cubic-shaped SAPO-47 crystals are obtained (size 260 μm×260 μm), at a synthesis temperature of 200 °C with a crystallization of 50 h.",

keywords = "One-step temperature process, SAPO-47, Single crystals, n-Propylamine",

author = "Xu, \{X. T.\} and Zhai, \{J. P.\} and Chen, \{Y. P.\} and Li, \{I. L.\} and Ruan, \{S. C.\} and Tang, \{Z. K.\}",

year = "2015",

month = jun,

day = "22",

doi = "10.1016/j.jcrysgro.2015.05.029",

language = "English",

volume = "426",

pages = "123--128",

journal = "Journal of Crystal Growth",

issn = "0022-0248",

publisher = "Elsevier B.V.",

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TY - JOUR

T1 - Synthesis of large optically clear SAPO-47 single crystals using n-propylamine as template

AU - Xu, X. T.

AU - Zhai, J. P.

AU - Chen, Y. P.

AU - Li, I. L.

AU - Ruan, S. C.

AU - Tang, Z. K.

PY - 2015/6/22

Y1 - 2015/6/22

N2 - We report the hydrothermal synthesis of SAPO-47 crystals by using n-propylamine (NPA) as template. The resulting product sensitively depends on the gel compositions and synthesis procedure. By optimizing the molar ratio of SiO2/Al2O3, content of HF and NPA, large perfect cubic-shaped SAPO-47 crystals are obtained (size 260 μm×260 μm), at a synthesis temperature of 200 °C with a crystallization of 50 h.

AB - We report the hydrothermal synthesis of SAPO-47 crystals by using n-propylamine (NPA) as template. The resulting product sensitively depends on the gel compositions and synthesis procedure. By optimizing the molar ratio of SiO2/Al2O3, content of HF and NPA, large perfect cubic-shaped SAPO-47 crystals are obtained (size 260 μm×260 μm), at a synthesis temperature of 200 °C with a crystallization of 50 h.

KW - One-step temperature process

KW - SAPO-47

KW - Single crystals

KW - n-Propylamine

UR - https://www.webofscience.com/wos/woscc/full-record/WOS:000358745700019

UR - https://openalex.org/W566197618

UR - https://www.scopus.com/pages/publications/84934974047

U2 - 10.1016/j.jcrysgro.2015.05.029

DO - 10.1016/j.jcrysgro.2015.05.029

M3 - Journal Article

SN - 0022-0248

VL - 426

SP - 123

EP - 128

JO - Journal of Crystal Growth

JF - Journal of Crystal Growth

ER -

Synthesis of large optically clear SAPO-47 single crystals using n-propylamine as template

Abstract

Bibliographical note

Keywords

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